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J. Vac. Sci. Technol. B 26, 2179 (2008); http://dx.doi.org/10.1116/1.2968613 (4 pages)

Fabrication of 200 nm period blazed transmission gratings on silicon-on-insulator wafers

Minseung Ahn, Ralf K. Heilmann, and Mark L. Schattenburg

Massachusetts Institute of Technology, Cambridge, Massachusetts 02139

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(Published online 1 December 2008)

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The authors report on the fabrication of 200 nm period blazed transmission gratings on silicon-on-insulator (SOI) wafers. These critical angle transmission (CAT) gratings require 3–5 μm tall freestanding grating bars with a very high aspect ratio (>100) and smooth sidewalls. In order to meet the challenging geometrical requirements, they modified and improved our previously reported process for the fabrication of a CAT grating prototype with 574 nm period. They have used potassium hydroxide (KOH) solutions to fabricate high aspect ratio gratings on ⟨110⟩ SOI wafers. The KOH etching process was improved to minimize the lateral undercut through precise grating alignment to ⟨111⟩ planes within ±0.05° and a room temperature etch process with 50 wt % KOH. In addition, an image-reversal technique with a high silicon content spin-on polymer was applied to increase process latitude with a high duty cycle nitride mask. A surfactant was also added to the KOH solution to promote hydrogen bubble release. With the improved process, they achieved a high etch anisotropy of above 300 on a ⟨110⟩ silicon wafer. They successfully fabricated 200 nm period CAT gratings with support mesh periods of 25 and 40 μm in a 9 mm2 area of 4-μm-thick silicon membranes on ⟨110⟩ SOI wafers.

© 2008 American Vacuum Society

ACKNOWLEDGMENTS

The authors gratefully acknowledge the assistance of Robert Fleming and Chih-Hao Chang of the MIT Space Nanotechnology Laboratory and James Daley of the MIT NanoStructures Laboratory. Staff and facility support from the Space Nanotechnology Laboratory, NanoStructures Laboratory, and Microsystems Technology Laboratories at MIT are also appreciated. This work is supported by NASA Grant No. NNX07AG98G, Kavli Instrumentation and Technology Development Fund, and a Samsung Scholarship.

Article Outline

  1. INTRODUCTION
  2. FABRICATION
  3. RESULTS AND DISCUSSION
  4. CONCLUSION AND FUTURE WORK

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1071-1023 (print)  
1520-8567 (online)

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